Large Scale Chemical Distillation Equipment With Optional External Condenser

20L - 50L Reboiler Fractional Distillation Column for CBD / THC / Hemp oil

——Operation

Feed liquid is admitted into still under high vacuum, immediately spread into a very thin film and forced quickly down the evaporation surface. Heated walls and high vacuum drive the more volatile components (distillate) to the external condenser as the less volatile components (residue) continue down the cylinder. The resulting fractions, thus separated, exit through individual discharge outlets. Depending on application, the desired product is either the distillate or the residue fraction. Small amounts of condensable low MW compounds collect in cold trap upstream of vacuum system. For high solvent loads, an optional external condenser may be installed immediately downstream of the still.

Large-scale industrial Fractional Distillation Columns use reflux to achieve a more complete separation of products. Reflux refers to the portion of the condensed overhead liquid product from a distillation or fractionation tower that is returned to the upper part of the tower as shown in the schematic diagram of a typical, large-scale industrial Fractional Distillation Column. Inside the Fractional Distillation Column, the reflux liquid flowing downwards provides the cooling needed to condense the vapors flowing upwards, thereby increasing the effectiveness of the distillation tower. The more reflux is provided for a given number of theoretical plates, the better the tower's separation of lower boiling materials from higher boiling materials. Alternatively, the more reflux provided for a given desired separation, the fewer theoretical plates are required.